Journal
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
Volume 191, Issue 11-12, Pages 1658-1659Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/10426507.2016.1225061
Keywords
Catalysis; C-H functionalization; dialkyl-H-phosphonate; electrochemical oxidation; hetaryl-azoles; salts of transition metals
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Funding
- Russian Science Foundation [14-23-00016] Funding Source: Russian Science Foundation
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Metal-catalyzed electrochemical oxidative phosphonation of hetaryl-azoles (benzoxazoles, benzothiazole and others) with dialkyl-H-phosphonate was developed. Joint electrochemical oxidation of azoles and dialkyl-H-phosphonate mixtures in the presence of catalytic quantities of salts of transition metals at room temperature affords the desired 2-substituted azoles. Palladium, nickel and silver salts were tested as catalysts. [GRAPHICS] .
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