Journal
ORGANIC LETTERS
Volume 18, Issue 9, Pages 2264-2267Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b00902
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Funding
- National Science Foundation of China [21272267]
- State Key Laboratory of Heavy Oil Processing [SKLOP201401001]
- Beijing National Laboratory for Molecular Sciences (BNLMS)
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An iron-catalyzed radical [2 + 2 + 2] annulation of benzene-linked 1,7-enynes with aldehydes has been developed. With this method, a variety of fused [6.6.6] pyran molecules are built in an efficient and selective manner. The aldehydic radical-mediated strategy exhibits a particularly attractive dual role, which triggers and terminates the domino cyclization.
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