Journal
ORGANIC LETTERS
Volume 18, Issue 17, Pages 4296-4299Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b02048
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Funding
- Deutsche Forschungsgemeinschaft [SFB 1083]
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Ethynylcyclooctynes and diazides were synthesized and applied for a chemoselective sequence of copper(I)-catalyzed azide-alkyne cycloadditions and strain-promoted azide alkyne cycloadditions. Chemoselectivity within the reaction sequence was achieved by balancing three factors: Cu-catalysis/ring strain/steric shielding. A cholic acid derived triazide was subjected to the cycloaddition sequence as a model system for a layer-by-layer synthesis on surfaces.
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