Journal
ORGANIC LETTERS
Volume 18, Issue 23, Pages 6180-6183Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b03223
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An efficient photoredox/Ni dual catalytic C-sp(2-) C-sp(3) cross-coupling protocol in a continuous-flow regime to synthesize a variety of regioisomeric cycloalkyl substituted 7-azaindoles has been developed. These transformations proceed efficiently under mild conditions (blue LED light irradiation at 30 degrees C over 40 min residence time in mixed solvent systems). Reactions are easy to perform and afford most of the desired 2-, 3-, 4-, 5-, and 6-cycloalkyl substituted 7-azaindoles in moderate to-good yield.
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