Journal
ORGANIC LETTERS
Volume 18, Issue 9, Pages 2280-2283Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b00878
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Funding
- China NSFC [21272047, 21372055, 21472030]
- SKLUWRE [2015DX01]
- Fundamental Research Funds for the Central Universities [HIT.BRETIV.201310]
- HLJNSF [B201406]
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A novel photochemical approach for the synthesis of phenanthrene derivatives from linear 3-aryl-N-(arylsulfonyl) propiolamides via a tandem radical Smiles rearrangement/C-S bonding/Mallory reaction is disclosed. The control experiment results and isolation of the key intermediates give further insight into the reaction mechanism. Gram scale reaction using a flow reactor demonstrated the synthetic potential applications of our protocol.
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