Journal
ORGANIC LETTERS
Volume 18, Issue 12, Pages 2962-2965Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b01301
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Funding
- National Natural Science Foundation of China [21472084, 81421091]
- Qing Lan Project of Jiangsu Province
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An electron-donor acceptor (EDA) complex between Togni's reagent and a tertiary amine has been introduced. The existence of this EDA complex was supported by NMR titration experiments. The hydrotrifluoromethylation of unactivated aliphatic alkenes and alkynes enabled by this EDA complex has also been developed. This hydrotrifluoromethylation protocol is operationally simple and, promoted by a tertiary amine.
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