Journal
ORGANIC LETTERS
Volume 18, Issue 11, Pages 2640-2643Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b01073
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Funding
- National Natural Science Foundation of China [21232004, 21472123, 21572131]
- Science and Technology Commission of Shanghai Municipality [14XD1402300]
- China Postdoctoral Science Foundation [2014M551397]
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Via a strategy of asymmetric reductive desymmetrization, chiral cis-epoxy naphthoquinols with multiple contiguous stereocenters and functional groups Were synthesized with excellent enantioselectivities (96-99% ee) and diastereoselectivities (8/1-15/1). A combined asymmetric hydrogenation/transfer hydrogenation mechanism was proposed based on experimental results.
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