Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 14, Issue 8, Pages 2413-2420Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ob02405f
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Funding
- National Natural Science Foundation of China [21572075, 21172085]
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A one-pot synthesis of 1H-isochromenes and 1,2-dihydroisoquinolines by a I-MCR/Wittig sequence was developed. The reaction of phosphonium salt 5, an acid, an amine ( or without), and an isocyanide gave the 1H-isochromenes 7 or 1,2-dihydroisoquinolines 9 in good yields by a sequential Passerini or Ugi condensation and an intramolecular Wittig reaction in the presence of K2CO3.
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