Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 14, Issue 31, Pages 7463-7467Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ob01352j
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Funding
- National Natural Science Foundation of China [21402144, 21372181, 21572168]
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A highly practical copper-catalyzed intermolecular chloroazidation of alpha,beta-unsaturated amides has been described, giving a series of azidochlorides in good-to-excellent yields. The stable azidoiodine (III) reagent and SOCl2 were used as azide and chlorine sources, respectively. The synthetic applications of this protocol were also explored by a variety of synthetically useful transformations.
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