Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 357, Issue 5, Pages 987-992Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201400801
Keywords
metal-free conditions; molecular iodine; S-N bond formation; sodium sulfinates; sulfonamides
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Funding
- National Natural Science Foundation of China [21302109, 21302110, 21375075]
- Taishan Scholar Foundation of Shandong Province
- Excellent Middle-Aged and Young Scientist Award Foundation of Shandong Province [BS2013YY019]
- Scientific Research Foundation of Qufu Normal University [BSQD 2012020]
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A simple, practical, and metal-free protocol has been developed for the synthesis of sulfonamides from sodium sulfinates and various amines through an iodine-mediated S-N bond formation reaction at room temperature. This green reaction is cost-effective, operationally straightforward, and especially proceeds under very mild conditions to afford the target products in good to excellent yields (up to 98%).
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