Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 357, Issue 16-17, Pages 3479-3484Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201500645
Keywords
1,2-diaza-1,3-dienes; 4,5-dihydropyridazin-3(2H)-ones; isothiourea catalysis
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Funding
- National Natural Science Foundation of China [NSFC21272276, NSFC21502232]
- Natural Science Foundation of Jiangsu Province [BK20140655]
- Foundation of State Key Laboratory of Natural Medicines [ZZJQ201306]
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An unprecedented [4+2] cycloaddition of in situ generated azoalkenes with arylacetic acids has been developed under the catalysis of isothiourea. The reaction provided an efficient approach to the synthesis of 4,5-dihydropyridazin-3(2H)-one derivatives in moderate to good yields (up to 95%).
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