3.8 Article

Synthesis and crystal structures of (E)-N'-(4-chloro-3-nitrobenzylidene)acetohydrazide and (E)-2-(4-chlorobenzylidene)-1-(quinolin-8-yl)hydrazine

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INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S2056989023006412

Keywords

synthesis; crystal structure; benzylidene; hydrazine

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The syntheses and structural characterization of two benzylidenehydrazine derivatives were reported. The properties of the molecules were characterized using various analytical techniques, and their structures were determined by single-crystal X-ray diffraction.
The syntheses of two benzylidenehydrazine derivatives, namely, (E)-N'-(4'-chloro-3-nitrobenzylidene)acetohydrazide, C9H8ClN3O3, and (E)-2-(4-chloro-benzylidene)-1-(quinolin-8-yl)hydrazine, C16H12ClN3, are reported. The molecules have been characterized using IR, H-1 NMR, C-13 NMR and mass spectroscopic and elemental analysis techniques, and their structures have been determined by single-crystal X-ray diffraction.

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