Journal
MOLBANK
Volume 2023, Issue 3, Pages -Publisher
MDPI
DOI: 10.3390/M1718
Keywords
2-fluoronitrobenzene; nucleophilic aromatic substitution; aromatic nitro group reduction
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In this study, a monosubstituted benzene-1,2-diamine building block was prepared in two steps from commercially available compounds, and two new compounds were successfully synthesized.
A monosubstituted benzene-1,2-diamine building block, N1-(3,5-bis(trifluoromethyl)benzyl)benzene-1,2-diamine, was prepared in two steps from commercially available 3,5-bis(trifluoromethyl)benzylamine and 1-fluoro-2-nitrobenzene, while the use of 3,5-bis(trifluoromethyl)aniline as the starting amine gave a triarylamine, N,N-bis(2-nitrophenyl)-3,5-bis(trifluoromethyl)aniline. The structures of the newly synthesized compounds were fully characterized.
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