Journal
APPLIED SCIENCES-BASEL
Volume 13, Issue 21, Pages -Publisher
MDPI
DOI: 10.3390/app132111864
Keywords
Q-Tube; Mg-Al hydrotalcite; aza-Michael addition reaction; chalcone; aminoazoles; fused azines
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An efficient, economical, and green synthesis method for fused azines has been developed using Mg-Al hydrotalcite under a high-pressure Q-Tube reactor. This method offers short reaction time, excellent yields, and the ability to reuse the catalyst without losing its catalytic activity for multiple cycles.
An efficient, economical, and green, sustainable synthesis of fused azines using Mg-Al hydrotalcite under a high-pressure Q-Tube reactor has been developed. This reaction proceeds through the aza-Michael addition of alpha,beta-unsaturated ketone with different aminoazoles. This method offered excellent yields in a short reaction time that economically saved energy in addition to the protocol showing the reuse of the catalyst seven times without losing its catalytic activity.
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