4.5 Article

Phenanthro[9,10-d ]imidazoles: An Unexpected Synthetic Route

Journal

SYNTHESIS-STUTTGART
Volume -, Issue -, Pages -

Publisher

GEORG THIEME VERLAG KG
DOI: 10.1055/s-0042-1751493

Keywords

azides; fragmentations; amines; heterocycles; amides

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A new synthetic route for phenanthro[9,10-d]imidazoles is reported. The target compounds were synthesized through the aminolysis of readily accessible 10,10-diazidophenanthren-9(10H)-one with nucleophilic amines, followed by a self-condensation. X-ray single crystallography was used to determine the molecular structures, and the optical properties of the material were described.
A new synthetic route for the synthesis of phenanthro[9,10-d]imidazoles is described. Through aminolysis of easily accessible 10,10-diazidophenanthren-9(10H)-one with nucleophilic amines, a self-condensation is triggered that results in the formation of the target phenanthro[9,10-d]imidazoles. The molecular structures were studied by X-ray single crystallography, and the optical properties of the material are described.

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