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Recent advances in self-healing superhydrophobic coatings

NANO TODAY (2023)

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Multifunctional coating on magnesium alloy: Superhydrophobic, self-healing, anti-corrosion and wear-resistant

Niumeng Huang et al.

Summary: Superhydrophobic coating (SHC) was prepared on magnesium (Mg) alloy through sequential surface etching, in-situ growth of Mg-Al-layered double hydroxides (LDHs), and modification of octadecyl-trimethoxy-silane (OTMS). The fabricated SHC exhibited contact angles above 150 degrees and sliding angles below 10 degrees when exposed to acidic or alkaline solutions, such as HCl, NaOH, NaCl, as well as milk, cola, and tea. The SHC significantly improved lubrication and wear resistance compared to the bare Mg alloy. Furthermore, the corrosion of Mg alloy was greatly reduced by the SHC, which maintained long-term hydrophobicity even after immersion in NaCl solution for 6 weeks. Any scratches on the SHC could self-heal within 8 days by immersing in water, thanks to the hydrolytic polycondensation of silane and corrosion decomposition of LDHs.

SURFACE & COATINGS TECHNOLOGY (2023)

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Self-healing and anticorrosion coatings based on responsive polymers with metal coordination bonds

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Summary: A new smart coating has been developed that can selectively release corrosion inhibitors and autonomously repair mechanical damages. This coating shows great potential in inhibiting metal corrosion and restoring anticorrosion properties.

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Design of Organic-Free Superhydrophobic TiO2 with Ultraviolet Stability or Ultraviolet-Induced Switchable Wettability

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Summary: This research successfully developed superhydrophobic TiO2 nanoparticles with ultraviolet stability and reversible wetting transition using pulsed chemical vapor deposition. Experimental and simulation studies revealed that the adsorption characteristics of surface oxygen vacancies and the resistance of dense amorphous TiO2 film to electron and hole migration are crucial for achieving superhydrophobic properties.

ACS APPLIED MATERIALS & INTERFACES (2022)

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Processing of Self-Healing Polymers for Soft Robotics

Ellen Roels et al.

Summary: Self-healing soft robots can recover completely from damage and have an extended lifetime, with various techniques used to shape complex structures. Reversible covalent and chemical cross-links provide healing abilities to soft robotic components, addressing current obstacles in soft robotics.

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Self-healing concrete for sustainable buildings. A review

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Self-roughened superhydrophobic polydopamine coating with excellent self-cleaning, anti-corrosion, and UV shielding performances

Jianfei Yang et al.

Summary: A hierarchical superhydrophobic PDA coating was fabricated on a copper substrate using a self-assembly method, which exhibits excellent self-cleaning performance, enhanced corrosion resistance, and additional functions of UV resistance and self-healing. PDA and the surface modifier are environmentally friendly and biodegradable.

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Polyurethane Blended with Silica-Nanoparticle-Modified Graphene as a Flexible and Superhydrophobic Conductive Coating with a Self-Healing Ability for Sensing Applications

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Summary: In this study, a flexible and superhydrophobic nanocomposite coating with dual self-healing ability was prepared. The coating exhibits intrinsic self-healing ability through disulfide bonds and multiple hydrogen bonds, and also has superficial self-healing ability through migration of hydrophobic long chains. The multifunctional coating shows excellent piezoresistive sensing performance and superhydrophobic ability, making it suitable for applications in antistatic electricity, wearable electronics, battery, electromagnetic shielding, and more.

ACS APPLIED NANO MATERIALS (2022)

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Near infrared light responsive surface with self-healing superhydrophobicity in surface chemistry and microstructure

Yacong Hou et al.

Summary: This study demonstrates a high-efficiency self-healing hydrophobic surface with remote control ability. By using near infrared light irradiation, the collapsed surface microstructure and altered surface chemistry can be easily recovered in a short period of time. The surface has great potential and broad impacts due to its simplicity and efficiency.

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Superhydrophobic polyurethane sponge based on sepiolite for efficient oil/water separation

Yao Pang et al.

Summary: In this study, micro-nan silica grown from the surface of fibrous sepiolite was organically modified and combined with oily epoxy resin to prepare a superhydrophobic polyurethane sponge. The sponge exhibited excellent oil-water separation performance, strong resistance to corrosion, and good mechanical stability.

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Fast Self-Healing and Self-Cleaning Anticorrosion Coating Based on Dynamic Reversible Imine and Multiple Hydrogen Bonds

Pingjing Mo et al.

Summary: In this study, a multifunctional coating material with excellent anticorrosion performance, fast self-healing, and self-cleaning properties is reported. The PDMS-TA-PUa coating, which is modified with a double reversible dynamic bond crosslinking network structure, can repair cracks within 40-50 minutes at room temperature.

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Fast self-healing and antifouling polyurethane/fluorinated polysiloxane-microcapsules-silica composite material

Jie Liu et al.

Summary: In this study, a fast self-healing and antifouling composite material called PFPMS was prepared. It exhibited excellent mechanical and antifouling properties, and achieved fast self-healing through the cross-linking reaction of ruptured microcapsules. The micro-nano-dual-scale surface formed by the microcapsules and nano-SiO2 contributed to the superior antifouling performance of PFPMS.

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Thermally induced response self-healing superhydrophobic wood with self-cleaning and photocatalytic performance

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Summary: The research focuses on the rational assembly of superhydrophobic coatings on wood fibers, making the wood possess superhydrophobicity, self-healing, self-cleaning, and photocatalytic properties, which has promising applications.

CELLULOSE (2022)

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A superhydrophobic carbon nanotube hollow fiber membrane for electrically self-heating membrane distillation

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Ultrafast Self-Healing Superhydrophobic Surface for Underwater Drag Reduction

Pengfei Sun et al.

Summary: A superhydrophobic surface with ultrafast repairability was developed for drag reduction in water. The addition of porous structures improves the drag reduction rate to 76%.

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Robust photothermal self-healing superhydrophobic coating based on carbon nanosphere/carbon nanotube composite

Yiqi Ma et al.

Summary: In this study, a photothermal superhydrophobic surface was fabricated using carbon nanospheres/carbon nanotubes (CNSs/CNTs) composite, and its self-healing effect under solar irradiation was demonstrated. The coating exhibited excellent superhydrophobic properties with a water contact angle of 160.7 degrees and sliding angle of 4.0 degrees, and could convert light energy into heat energy efficiently. The self-healing mechanism of the coating was found to involve the migration of hydrophobic long chains under thermodynamic drive.

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Functional and versatile colorful superhydrophobic nanocellulose-based membrane with high durability, high-efficiency oil/water separation and oil spill cleanup

Zuozhu Yin et al.

Summary: This translation introduces a one-step spraying method for fabricating a colorful superhydrophobic nanocellulose-based membrane with high durability and efficiency in oil/water separation and oil spill cleanup. The dosage of pigment dispersions can regulate the color diversity and depth of the membrane. The membrane exhibits excellent resilience and superhydrophobicity even after severe testing, and it can be used for creating colorful paintings and separating oil/water mixtures efficiently.

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Near infrared light responsive surface with self-healing superhydrophobicity in surface chemistry and microstructure

Yacong Hou et al.

Summary: This article introduces a highly efficient self-healing hydrophobic surface that can be remotely controlled and rapidly restored through near infrared light, with good self-healing ability and broad application prospects.

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Underwater Drag Reduction and Buoyancy Enhancement on Biomimetic Antiabrasive Superhydrophobic Coatings

Zhaochang Wang et al.

Summary: The study presents an easily prepared superhydrophobic coating with excellent liquid repellency and resistance, suitable for a wide range of applications.

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Fabrication of Dual Self-Healing Multifunctional Coating Based on Multicompartment Microcapsules

Changyue Xu et al.

Summary: By utilizing the self-healing mechanism inspired by natural creatures, this study successfully prepared a dual self-healing multifunctional coating with thermal insulation, anti-reflection, and superhydrophobic properties. The use of phase change materials (PCMs) and titanium dioxide (TiO2) contributed to the intrinsic and superficial dual self-healing ability of the coating, guiding the fabrication of high-performance self-healing materials and promoting the long-term use of multifunctional coatings.

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Design of a Smart Self-Healing Coating with Multiple-Responsive Superhydrophobicity and Its Application in Antibiofouling and Antibacterial Abilities

Xingxing Ni et al.

Summary: This study developed a smart self-healing and superhydrophobic coating based on the combination of multi-responsive ZnO-encapsulated mesoporous polydopamine microspheres and silicone latex, which can achieve self-healing under UV, NIR, acid, or base stimuli and exhibit excellent environmental endurance. The coating features controllable release of healing agents and antibacterial functionalization, providing new possibilities for long-term applications.

ACS APPLIED MATERIALS & INTERFACES (2021)

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Article Engineering, Environmental

Mechanically robust, self-healing superhydrophobic anti-icing coatings based on a novel fluorinated polyurethane synthesized by a two-step thiol click reaction

Kang Fu et al.

Summary: The study synthesized a mechanically robust SiO2-FPU superhydrophobic coating on various substrates using a two-step thiol click reaction, which maintained superhydrophobicity under tests like sandpaper abrasion, tape peeling, and water dripping, and showed great icing-delaying performance. The novel preparation strategy and FPU-based coating provide a new perspective in surface protection.

CHEMICAL ENGINEERING JOURNAL (2021)

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Article Engineering, Environmental

Formation and anticorrosion properties of superhydrophobic zinc coatings on steel

N. A. Polyakov et al.

Summary: The study found that superhydrophobic zinc coatings can be formed by depositing zinc in a sulfate-acetate solution and treating with stearic acid, optimizing the electrodeposition conditions to maintain superhydrophobic properties under salt spray conditions, and enhancing superhydrophobic properties with ultrasonic treatment.

CHEMICAL ENGINEERING JOURNAL (2021)

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Article Engineering, Chemical

Fabrication of robust green superhydrophobic hybrid nanofiber-nanosphere membrane for membrane distillation

Jiaxin Guo et al.

Summary: In this study, an innovative biaxial electrospinning technology was used to prepare a green superhydrophobic, monolayer hybrid membrane without the use of long-chain perfluorinated additives, achieving a superhydrophobic surface and good stability. The introduction of nanospheres reduced pore size, improved tensile strength, and reduced thermal conductivity, leading to higher liquid entry pressure (LEP) value and average water flux. Additionally, optical coherence tomography technology was employed to monitor foulant growth on the membrane surface in real-time during membrane distillation testing, demonstrating the exceptional long-term performance of the membrane.

DESALINATION (2021)

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Article Chemistry, Multidisciplinary

Constructing Scalable Superhydrophobic Membranes for Ultrafast Water-Oil Separation

Xi Quan Cheng et al.

Summary: A simple method of coaxial electrospinning was proposed to manufacture superhydrophobic membranes for ultrafast separation of water-in-oil emulsions. By designing asymmetric composite membranes with selective layers, the mass transfer resistance was reduced, resulting in high separation efficiency and permeance. The manufactured membrane showed strong promise in separation of water-in-oil emulsions, with a large size, continuous production, and potential for further enlargement.

ACS NANO (2021)

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Article Engineering, Environmental

An eco-friendly smart self-healing coating with NIR and pH dual-responsive superhydrophobic properties based on biomimetic stimuli-responsive mesoporous polydopamine microspheres

Xingxing Ni et al.

Summary: This study successfully fabricated a smart self-healing coating with near infrared and pH dual-responsive properties using a green synthesis method. The coating can self-heal its performance when damaged by external environment, possess anti-biofouling properties, and exhibit good stability in harsh conditions.

CHEMICAL ENGINEERING JOURNAL (2021)

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Superhydrophobic Coatings with Photothermal Self-Healing Chemical Composition and Microstructure for Efficient Corrosion Protection of Magnesium Alloy

Jiaojiao Zhang et al.

Summary: The study introduces a superhydrophobic self-healing coating with photothermal chemical composition and microstructure for the corrosion protection of magnesium alloy. The coating exhibits good superhydrophobicity, photothermal effect, and corrosion resistance, and demonstrates excellent self-healing capability in response to chemical and microstructure damage.

LANGMUIR (2021)

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Article Chemistry, Physical

Durable superhydrophobic cotton fabrics prepared by surface-initiated electrochemically mediated ATRP of polyhedral vinylsilsesquioxane and subsequent fluorination via thiol-Michael addition reaction

Hui Li et al.

Summary: Fluorinated polyhedral oligomeric silsesquioxane (F-POSS) is a popular candidate for superhydrophobic coating due to its ultralow surface energy. By grafting methacryl POSS (MA-POSS) onto cotton and subsequently reacting it with 1H, 1H, 2H, 2H-perfluorododecyl-1-thiol (PFDT), a durable poly(MA-POSS)-PFDT coating was fabricated with improved water resistance and abrasion resistance.

JOURNAL OF COLLOID AND INTERFACE SCIENCE (2021)

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Article Materials Science, Multidisciplinary

Self-healing behavior of epoxy-based double-layer nanocomposite coatings modified with Zirconia nanoparticles

Sehrish Habib et al.

Summary: This study investigates the self-healing behavior of epoxy-based double-layer nanocomposite coatings designed to mitigate corrosion, by loading zirconia nanoparticles, IM, and PEI to improve corrosion resistance performance. The release of loaded IM and PEI in response to external stimuli contributes to the enhanced corrosion resistance, making these coatings potentially valuable for oil & gas and marine applications.

MATERIALS & DESIGN (2021)

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Article Nanoscience & Nanotechnology

Improving Anti-Icing and De-Icing Performances via Thermal-Regulation with Macroporous Xerogel

Bo Yu et al.

Summary: The study demonstrates a new strategy for delaying icing and efficient de-icing using a superhydrophobic photothermal and thermal isolation macroporous xerogel (PMX).

ACS APPLIED MATERIALS & INTERFACES (2021)

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Article Chemistry, Applied

Topological cyclodextrin nanoparticles as crosslinkers for self-healing tough hydrogels as strain sensors

Junmin Chen et al.

Summary: Novel cyclodextrin topological nanoparticles have been developed with excellent crosslinking capabilities for the design of high stretchable, high-strength, and anti-fatigue hydrogels. These hydrogels can be used as flexible strain sensors to monitor human activities and can be readily recycled for reuse.

CARBOHYDRATE POLYMERS (2021)

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A Superhydrophobic Hydrogel for Self-Healing and Robust Strain Sensor with Liquid Impalement Resistance

Peng Wang et al.

Summary: The study successfully developed a superhydrophobic strain sensor with self-healing capability, mechanical robustness, and liquid impalement resistance, achieved by partially embedding hydrophobic graphene and carbon nanotubes into the hydrogel matrix, enabling accurate and real-time monitoring of human motion.

CHINESE JOURNAL OF CHEMISTRY (2021)

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Article Materials Science, Multidisciplinary

Monolithic polymeric porous superhydrophobic material with pneumatic plastron stabilization for functionally durable drag reduction in blood-contacting biomedical applications

Jennifer Marlena et al.

Summary: The study introduces a functional material that extends the functional durability of superhydrophobic slip flow through simple modifications on porous materials, enabling resistance to high pressure fluids and protein fouling, while controlling pore pressure within a wide range of applied pressures.

NPG ASIA MATERIALS (2021)

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Preparation and Properties of Self-Healing Waterborne Polyurethane Based on Dynamic Disulfide Bond

Gongbo Ye et al.

Summary: The self-healing waterborne polyurethane material with dynamic disulfide bond exhibited excellent stability and small particle size; Chemical characteristics were confirmed through FTIR and XPS tests; Self-healing efficiency reached 96.14% after heat treatment, with a reprocessed film tensile strength of 3.39 MPa.

POLYMERS (2021)

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Bioinspired in situ repeatable self-recovery of superhydrophobicity by self-reconstructing the hierarchical surface structure

Md Ahsan Habib et al.

Summary: Inspired by the biological self-recovery mechanism of superhydrophobicity, a new class of waxgel material has been reported, which features sustainable hierarchical surface micro-structures and the ability to self-reconstruct its surface layer after damage or removal. This material does not require external input for self-recovery and exhibits durability and non-fluorinated composition.

CHEMICAL COMMUNICATIONS (2021)

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Large-scale fabrication of a durable and self-healing super-hydrophobic coating with high thermal stability and long-term corrosion resistance

Dawei Li et al.

Summary: A durable superhydrophobic coating was prepared using a fluorine-free suspension, exhibiting outstanding wettability and durability. It showed excellent resistance to high and low temperatures, UV radiation, chemical attack, and mechanical tests, with repairable ability and self-cleaning properties even after damage. The influence of multiple hybridizations on the coating's long-term corrosion stability and thermal properties was systematically studied, showing promising application prospects.

NANOSCALE (2021)

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Injectable, self-healing mesoporous silica nanocomposite hydrogels with improved mechanical properties

A. Zengin et al.

Summary: By chemically crosslinking thiol-functionalized mesoporous silica nanoparticles with hydrophilic polymers such as polyethylene glycol, nanocomposites with high storage modulus and rapid self-healing capabilities were successfully formed. This approach offers a promising strategy to create multifunctional self-healing biomaterials for a wider range of applications in regenerative medicine.

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Superhydrophobic Self-Healing Coatings Comprised of Hemispherical Particles Arrays Decorated by Fluorocarbon-Coated Nanoscale Fe2O3 Rods and SiO2 Particles

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