4.7 Article

Creep deformation behaviour of thermomechanically treated India specific re duce d activation ferritic martensitic steel

Journal

JOURNAL OF NUCLEAR MATERIALS
Volume 581, Issue -, Pages -

Publisher

ELSEVIER
DOI: 10.1016/j.jnucmat.2023.154441

Keywords

INRAFM steel; Thermomechanical treatment; Creep properties; M 23 C 6 and MX precipitates

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The present study investigated the influence of thermomechanical treatment (TMT) on the microstructural evolution and creep deformation behavior of India specific reduced activation ferritic martensitic (INRAFM) steel. TMT treated steel showed refinement in lath structure and an increase in the population of finer precipitates, leading to enhanced creep resistance. Norton's power law was used to describe the dependence of minimum creep rate on applied stress, and the modified Monkman-Grant relation showed a good correlation between rupture time/strain to failure and minimum creep rate. TMT treated steel also exhibited lower rate of exhaustion, higher threshold stress, and prolonged tertiary creep region.
In the present work, the influence of thermomechanical treatment (TMT) on microstructural evolution and creep deformation behaviour of India specific reduced activation ferritic martensitic (INRAFM) steel was investigated. Firstly, the TMT was carried out on INRAFM steel by reducing its thickness to 25% at warm rolling temperature (973 K), followed by tempering for 90 min at 1033 K. The resultant microstructural characteristics were compared with those attained in normalized and tempered (N + T) condition. TMT treated steel shows a refinement in lath structure with an increment in population of finer M 23 C 6 precipitates along the hierarchal PAG/packet/block boundaries and MX carbonitrides in the intralath region. After TMT, creep tests were performed on the steel over the stress range of 20 0-30 0 MPa at temperature of 823 K. The rupture time of the steel significantly increased upon TMT, due to refinement in microstructural features that enhanced the creep resistance. Dependence of minimum creep rate on applied stress obeys Norton's power law and the stress exponent values indicated the deformation mechanism as dislocation creep. Modified Monkman-Grant relation shows a good relation between rupture time/strain to failure with minimum creep rate. Thereafter, the effect of TMT on the transient, secondary and tertiary creep behaviour was also examined and presented in this work. The TMT treated steel shows lower rate of exhaustion, higher threshold stress and prolonged tertiary region. & COPY; 2023 Elsevier B.V. All rights reserved.

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