Journal
CHEMICAL COMMUNICATIONS
Volume 51, Issue 92, Pages 16573-16576Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc06069a
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Funding
- National Natural Science Foundation of China [91127041, 21172045, 21572036]
- Changjiang Scholars and Innovative Research Team in University [IRT1117]
- Shanghai International Cooperation Program [14230710600]
- Doctoral Fund of Ministry of Education of China [20130071110032]
- Department of Chemistry Fudan University
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By using O-benzoyl hydroxylamines as amine sources, the first convenient copper-catalyzed electrophilic amination of sodium sulfinates has been realized. Even with 2 mol% catalyst loading, the protocol provided an efficient and straightforward synthesis of a broad range of functional sulfonamides under ambient reaction conditions without an additional base and ligand. Based on the control experiments, a plausible mechanism was proposed.
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