4.7 Article

Sealed rotors for in situ high temperature high pressure MAS NMR

Journal

CHEMICAL COMMUNICATIONS
Volume 51, Issue 70, Pages 13458-13461

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc03910j

Keywords

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Funding

  1. U. S. Department of Energy (DOE), Office of Basic Energy Sciences, Division of Chemical Sciences, Geosciences Biosciences
  2. NIH Grant [NIEHS R01ES022176]
  3. DOE's Office of Biological and Environmental Research
  4. DOE [DE-AC06-76RLO1830]
  5. NATIONAL INSTITUTE OF ENVIRONMENTAL HEALTH SCIENCES [R01ES022176] Funding Source: NIH RePORTER

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Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.

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