Journal
CHEMICAL COMMUNICATIONS
Volume 51, Issue 34, Pages 7341-7344Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc01436k
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Funding
- National Basic Research Program of China [2015CB856600]
- NSFC [21422206, 21272206]
- Fundamental Research Funds for the Central Universities
- Zhejiang Provincial NSFC [LZ12B02001]
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The first nickel-catalyzed thiolation of unactivated C(sp(3))-H bonds with disulfides was described. This transformation uses (dppp) NiCl2 as a catalyst and BINOL as a ligand, which are efficient for the thiolation of beta-methyl C(sp(3))-H bonds of a broad range of aliphatic carboxamides. The reaction provides an efficient synthetic pathway to access diverse thioethers.
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