Journal
CHEMICAL COMMUNICATIONS
Volume 51, Issue 1, Pages 180-182Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc07938h
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Funding
- National Natural Science Foundation of China [21172038, 21372046]
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An unexpected result from the reaction of 2-alkynylaryldiazonium tetrafluoroborate with sulfur dioxide is described. In the presence of morpholin-4-amine, this transformation catalyzed by copper(I) bromide proceeds through insertion of sulfur dioxide and intramolecular 5-endo cyclization, leading to benzo[b]thiophene 1,1-dioxides in moderate to good yields.
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