Journal
CHEMICAL COMMUNICATIONS
Volume 51, Issue 25, Pages 5479-5481Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc08655d
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Funding
- National Basic Research Program of China [2012CB821600]
- National Natural Science Foundation of China [21372247, 21421002]
- SIOC
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An iron-mediated hydro-trifluoromethylthiolation of unactivated olefins under mild conditions was described for the first time. The reaction occurred to full conversion within 30 min at 0 degrees C and tolerates a variety of functional groups. Preliminary mechanistic studies suggested that the reaction proceeds via a free-radical pathway.
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