Journal
CHEMICAL COMMUNICATIONS
Volume 51, Issue 64, Pages 12851-12854Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc05048k
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Funding
- National Science Foundation [CHE-1151991, CHE-1308307]
- Ohio Board of Regents
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1308307] Funding Source: National Science Foundation
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1151991] Funding Source: National Science Foundation
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Mixing of metallocyclic trimers and tetramers in an exact 1 : 1.5 stoichiometry provided new supramolecular triangles in quantitative yields. Characterization of the new hetero-nuclear metallomacrocycles was achieved by H-1, 2D-COSY, 2D-NOESY, and C-13 NMR spectroscopy, along with ESI and TWIM mass spectrometry. Gradient tandem MS (gMS(2)) provided insight into the stabilities of the binuclear structures.
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