Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 365, Issue 19, Pages 3284-3289Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.202300632
Keywords
polyfluoroarenes; C(sp(2))-F bond cleavage; C(sp(3))-H polyfluoroarylation; radical-radical coupling; polyfluorinated diarylmethanes
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We have developed a visible light-induced transition metal-free benzylic C(sp(3))-C(sp(2)) defluorinative coupling reaction between indole derivatives and polyfluoroarenes via the sequential electron transfer-proton transfer (ET/PT) process, resulting in various polyfluorinated diarylmethanes. This protocol offers mild reaction conditions and good functional group tolerance.
A visible light-induced transition metal-free benzylic C(sp(3))-C(sp(2)) defluorinative coupling between indole derivatives and polyfluoroarenes via the sequential electron transfer-proton transfer (ET/PT) process has been developed, affording various polyfluorinated diarylmethanes. This protocol features mild conditions and good functional group tolerance.
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