Journal
MOLBANK
Volume 2023, Issue 2, Pages -Publisher
MDPI
DOI: 10.3390/M1636
Keywords
Lewis acid; Lewis base; 1; 3; 5-triaza-7-phosphaadmantane (PTA); carbenium ion; water solubility
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The novel organic salt was synthesized through a Lewis acid and Lewis-base reaction and analyzed by various spectroscopic and crystallographic techniques.
The novel organic salt 7-((5-bromo-1H-indol-3-yl)(4-methoxyphenyl)methyl)1,3,5-triaza-7-phosphaadamantan-7-ium tetrafluoroborate was synthesized from a Lewis acid (LA) and Lewis-base (LB) reaction between 1,3,5-triaza-7-phosphaadmantane (LB) and 5-bromo-3-(4-methoxybenzylidene)-3-H-indol-1-ium tetrafluoroborate (LA). The obtained Lewis acid base adduct, being the title compound, was analyzed and validated by H-1, C-13, P-31, and F-19 1D-NMR-spectroscopy, ESI mass spectrometry, CHN-elemental analysis, and a single crystal X-ray diffraction investigation.
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