4.7 Article

Microstructure evolution and mechanical properties of nano-SiCp/AZ91 composite processed by extrusion and equal channel angular pressing (ECAP)

Journal

MATERIALS CHARACTERIZATION
Volume 121, Issue -, Pages 222-230

Publisher

ELSEVIER SCIENCE INC
DOI: 10.1016/j.matchar.2016.10.003

Keywords

Magnesium matrix composite; Equal channel angular pressing (ECAP); Nano-scaled SiC particles; Agglomeration; Orowan strengthening

Funding

  1. Fundamental Research Funds for the Central Universities [HIT. NSRIF.2015003]
  2. National Natural Science Foundation of China [51301051]
  3. General Financial Grant from the China Postdoctoral Science Foundation [2013M531034]
  4. Special Financial Grant [2015T80344]
  5. Specialized Research Fund for the Doctoral Program of Higher Education [20132302120001]
  6. Heilongjiang Postdoctoral Foundation [LBH-Z13088]
  7. Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education Ministry

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Nano-SiCp/AZ91 magnesium matrix composite was fabricated by stir casting. The as-cast ingots were extruded at 350 degrees C, then processed by equal channel angular pressing (ECAP) at various temperatures (250 degrees C, 300 degrees C and 350 degrees C). Grains are significantly refined after the extrusion and the ECAP. A basal fibre texture was detected by neutron diffraction after the extrusion, which inclines about 45 degrees to the extrusion direction (ED) after the ECAP. Nano-scaled SiC particles agglomerate in the as-cast composite. After the extrusion, the agglomeration tends to form continuous or discontinuous strips along the extrusion direction. By application of the ECAP, the agglomerated SiC particles are partly dispersed and the strips formed during the extrusion tend to be thinner and broken with the increasing pass number. The yield tensile strength (YTS) and the ultimate tensile strength (UTS) of the composite are dramatically increased after the extrusion. ECAP for one pass at various temperatures further increases the strength, however, the YTS decreases with the increasing ECAP temperature and the pass number. The Orowan equations predict the maximum YTS of the composite may be up to 400 MPa providing SiC particles are homogenously distributed in the matrix. (C) 2016 Elsevier Inc. All rights reserved.

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