Journal
METALLOGRAPHY MICROSTRUCTURE AND ANALYSIS
Volume 12, Issue 3, Pages 427-432Publisher
SPRINGERNATURE
DOI: 10.1007/s13632-023-00945-3
Keywords
Pure zinc; KOBO extrusion; Point defect clusters; Modulated structure
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In the study of zinc subjected to severe plastic deformation at low temperature using the KOBO extrusion method, three techniques of micro and nanostructure identification (TEM, STEM, HAADF) were employed. It was found that the long trails pattern observed in the microstructure after KOBO deformation resulted from strain fields of densely spaced nano-sized point defect clusters (SIA clusters). The presence of satellite spots on the diffraction pattern was explained by a periodic arrangement of clusters forming a modulated lattice with a nano-sized wavelength.
In the study of plastic flow and mechanical features of zinc subjected to severe plastic deformation at low temperature through the KOBO extrusion method, three techniques of micro and nanostructure identification have been used (TEM, STEM, HAADF). It was shown that the pattern of long trails-a typical element of microstructure after the KOBO deformation, results from strain fields of densely spaced nano-dimensional clusters of point defects-SIA clusters. The presence of satellite spots on the diffraction pattern was explained by a periodic arrangement of clusters which takes the form of a modulated lattice with a nano-sized wavelength.
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