4.7 Article

Pore-induced defects during thermo-mechanical fatigue of a fourth-generation single crystal superalloy

Journal

MATERIALS RESEARCH LETTERS
Volume 11, Issue 8, Pages 678-687

Publisher

TAYLOR & FRANCIS INC
DOI: 10.1080/21663831.2023.2223558

Keywords

Fourth-generation single crystal superalloy; micro-pores; deformation twins; element segregation; thermo-mechanical fatigue

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Comparable investigation was conducted on pore-induced defects during in-phase (IP) and out-of-phase (OP) thermo-mechanical fatigue (TMF) in fourth-generation single crystal superalloy. It was found that recrystallizations and deformation twins formed near micro-pores in IP and OP cycling, respectively. High-resolution observation revealed that the increase of a/6(112) twinning dislocations and the more frequent activation of (112){111) viscous slipping during OP-TMF contributed to twinning nucleation. Atom-scale mapping further showed the dual effect of Re, Co, and Cr in promoting twinning formation and hindering partial dislocations movement. The accumulation of pore-induced twins was considered to cause premature fracture of the alloy during OP-TMF.
Comparable investigation of pore-induced defects during in-phase (IP) and out-of-phase (OP) thermo-mechanical fatigue (TMF) were conducted on fourth-generation single crystal superalloy. It was discovered that recrystallizations and deformation twins would take shape near micro-pores at IP and OP cycling, respectively. High-resolution observation uncovered that the increasing a/6(112) twinning dislocations and more frequent activation of (112){111) viscous slipping during OP-TMF accounted for twinning nucleation. Atom-scale mapping additionally disclosed the dual effect of Re, Co, and Cr in facilitating twinning formation and impeding of partial dislocations movement. It was deemed that the accumulation of pore-induced twins caused the premature fracture of alloy during OP-TMF.

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