A Detailed Analysis of the Microstructural Changes in the Vicinity of a Crack-Initiating Defect in Additively Manufactured AISI 316L

The fatigue life of metals manufactured via laser-based powder bed fusion (L-PBF) highly depends on process-induced defects. In this context, not only the size and geometry of the defect, but also the properties and the microstructure of the surrounding material volume must be considered. In the presented work, the microstructural changes in the vicinity of a crack-initiating defect in a fatigue specimen produced via L-PBF and made of AISI 316L were analyzed in detail. Xenon plasma focused ion beam (Xe-FIB) technique, scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD) were used to investigate the phase distribution, local misorientations, and grain structure, including the crystallographic orientations. These analyses revealed a fine grain structure in the vicinity of the defect, which is arranged in accordance with the melt pool geometry. Besides pronounced cyclic plastic deformation, a deformation-induced transformation of the initial austenitic phase into alpha'-martensite was observed. The plastic deformation as well as the phase transformation were more pronounced near the border between the defect and the surrounding material volume. However, the extent of the plastic deformation and the deformation-induced phase transformation varies locally in this border region. Although a beneficial effect of certain grain orientations on the phase transformation and plastic deformability was observed, the microstructural changes found cannot solely be explained by the respective crystallographic orientation. These changes are assumed to further depend on the inhomogeneous distribution of the multiaxial stresses beneath the defect as well as the grain morphology.

Automated summary

The fatigue life of metals manufactured via laser-based powder bed fusion (L-PBF) is affected by process-induced defects, including size, geometry, and material properties. In this study, the microstructural changes near a crack-initiating defect in an AISI 316L fatigue specimen produced via L-PBF were analyzed using Xe-FIB, SEM, and EBSD techniques. The analyses revealed a fine grain structure arranged according to the melt pool geometry. Plastic deformation and phase transformation were observed near the border between the defect and surrounding material, with localized variations. The microstructural changes cannot be solely explained by crystallographic orientation, but also depend on the distribution of multiaxial stresses and grain morphology.