4.5 Article

Phase Transformation Behaviors and Dislocation Evolutions of an Additively Manufactured Ti-6Al-4V Alloy under Annealing Treatment

Journal

METALS
Volume 13, Issue 6, Pages -

Publisher

MDPI
DOI: 10.3390/met13061061

Keywords

additive manufacturing; titanium alloy; heat treatment; phase transformation; dislocation; mechanical property

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Post annealing treatment was conducted on laser powder bed fusion-built Ti-6Al-4V alloy to study its phase transformation behaviors and dislocation evolutions. The results showed that post annealing treatment effectively decomposed martensitic and α' phases and eliminated dislocations. The martensite decomposition rate increased with the annealing temperature. Annealing at 700°C for 4 hours eliminated 98% of the dislocations, and further annealing had limited influence on the dislocation density. Annealing at 700°C for 16 hours resulted in a high ductility of 10.3% due to the favorable equilibrium lamellar α+β microstructure. These findings provide valuable insights for optimizing post annealing treatment procedures to enhance the mechanical properties of additively manufactured Ti-6Al-4V alloys.
Post annealing treatment is generally needed for additively manufactured titanium alloy to decompose metastable phases, alleviate residual stress, and improve ductility. In this work, in-situ electrical resistivity and line profile analysis of X-ray diffraction were utilized for monitoring phase transformation behaviors and dislocation evolutions of a laser powder bed fusion-built Ti-6Al-4V alloy under post annealing treatment. Besides, hardness and tensile tests were adopted for revealing the effects of phase transformation and dislocation evolutions on the mechanical properties. The results indicated that post annealing treatment decomposed martensitic & alpha;& PRIME; into lamellar & alpha; + & beta; and eliminated dislocations efficiently. The martensite decomposition rate increased with the annealing temperature. Annealing at 700 & DEG;C for 4 h eliminated 98% of the dislocations, and further annealing has only a limited influence on the dislocation density. Annealing at 700 & DEG;C for 16 h is beneficial for achieving a high ductility of 10.3% owing to the favorable equilibrium lamellar & alpha; + & beta; microstructure. These findings provide valuable insights for optimizing post annealing treatment procedures to enhance the mechanical properties of additively manufactured Ti-6Al-4V alloys.

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