Journal
POLYMERS
Volume 15, Issue 6, Pages -Publisher
MDPI
DOI: 10.3390/polym15061544
Keywords
pultrusion; simulation; closed injection pultrusion CIP; aliphatic polyurethane; thermoset; pressure development; ii-chamber
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The open bath impregnation method is enhanced to closed resin-injection pultrusion (CIP) for the use of innovative higher-performance resin systems. The study investigates the influence of resin viscosity, opening angle, and opening factor on the process pressures in the injection and impregnation chamber. A newly developed simulation model based on Darcy's law is validated using data obtained from pultrusion trials.
The use of innovative higher-performance highly reactive resin systems requires an enhancement of the established method of fiber impregnation (open bath) towards closed resin-injection pultrusion (CIP), due to the short pot life of the resin systems. The result is that the open bath is developed into a closed injection and impregnation chamber (ii-chamber). In this study, three parameters-resin viscosity, opening angle and opening factor at the injection point on the ii-chamber-are varied, each in three stages. For each set of parameters, a pultrusion trial is conducted and the process pressures in the ii-chamber and pultrusion die measured. This enables direct feedback via the process conditions of the as yet uncured composite. The data obtained are used to validate a newly developed simulation model. The model is based on Darcy's law, which has been extended to take fiber movement into account and thus represent the resulting pressure increase in the die. The flexible ii-chamber and die concept enhance our understanding of the processes taking place in the die system. The sensitivity of the process pressures can be shown for the three influencing variables. The experiment shows that of the three influencing variables investigated, viscosity has the greatest sensitivity to pressure development. In general, it can be said that over the length of the pultrusion die system, the pressure level increases across the three measuring points.
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