Journal
ORGANIC LETTERS
Volume -, Issue -, Pages -Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.3c00439
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This study describes a concise Fe-catalyzed alkylazidation of alpha-trifluormethylalkenes via a C-C bond cleavage/radical addition/azidation cascade. The protocol offers a practical and step-economic approach to the synthesis of tertiary alpha-trifluoromethyl azides, with broad substrate scope, excellent functional group compatibility, and the ability to be performed on a gram scale.
A concise Fe-catalyzed alkylazidation of alpha-trifluor-omethylalkenes via a C-C bond cleavage/radical addition/ azidation cascade is described. This protocol features a broad substrate scope, excellent functional group compatibility, and the ability to be performed on a gram scale, thus offering a practical and step-economic approach to the synthetically useful tertiary alpha- trifluoromethyl azides.
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