Journal
JOURNAL OF SOLID STATE CHEMISTRY
Volume 321, Issue -, Pages -Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jssc.2023.123918
Keywords
Tin-oxo clusters; Ligands effect; Contact angle; ElectrocatalyticCO2 reduction
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Two isostructural Sn5-oxo clusters, (nBuSn)5(mu 3-O)2(EG4)L3 (H2EG = ethylene glycol, L = 4-tert-butylbenzoate or 4-hydroxybenzoate), were successfully prepared using (nBuSn)OH2Cl as tin source pre-cursor. Comparative studies on contact angle test and electrocatalytic carbon dioxide reduction reveal that the 4-tert-butylbenzoate decorated Sn5 with a more hydrophobic surface shows higher catalytic activity.
Two Sn5-oxo clusters with isostructural cores, (nBuSn)5(mu 3-O)2(EG4)L3 (H2EG = ethylene glycol, L = 4-tert- butylbenzoate or 4-hydroxybenzoate), have been successfully prepared using (nBuSn)OH2Cl as tin source pre-cursor. Comparative studies of contact angle test and electrocatalytic carbon dioxide reduction reveal that the 4-tert-butylbenzoate decorated Sn5 with more hydrophobic surface possesses higher catalytic activity.
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