Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 88, Issue 11, Pages 7512-7517Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.3c00329
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In this study, the Ir(III)-catalyzed synthesis of 3-pyrrolidinols and 4-piperidinols by reacting 1,2,4-butanetriol or 1,3,5-pentanetriol with primary amines was demonstrated. This borrowing hydrogen methodology was also applied to the sequential diamination of triols, leading to the formation of amino-pyrrolidines and aminopiperidines.
The Ir(III)-catalyzed synthesis of 3-pyrrolidinols and 4-piperidinols combining 1,2,4-butanetriol or 1,3,5-pentanetriol with primary amines was carried out. This borrowing hydrogen methodology was further extended to the sequential diamination of triols leading to amino-pyrrolidines and aminopiperidines.
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