Journal
JOURNAL OF THE ELECTROCHEMICAL SOCIETY
Volume 163, Issue 6, Pages H434-H439Publisher
ELECTROCHEMICAL SOC INC
DOI: 10.1149/2.1041606jes
Keywords
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Funding
- National Research Lab program of National Research Foundation of Korea [NRF-2015R1A2A1A01006192]
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A branched TiO2/CdS nanorod core-shell structure with high surface area is fabricated on fluorine-doped tin oxide glass substrates by a cost-effective wet chemical method for use as a photoelectrode in the photoelectro-chemical production of hydrogen. The growth of a TiO2 nanorod array and subsequent finer TiO2 branches on the TiO2 nanorods form the basic three-dimensional hierarchical structure and is further coated with a CdS layer by the chemical bath deposition method. The morphologies and structures of the electrodes are characterized by X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The performance of the electrode is evaluated by measuring the photocurrent density, the applied-bias photo-to-electron current conversion efficiency, and the volume of hydrogen produced. The observed photocurrent density is 13 mA cm(-2), and the efficiency is 4.68%. A critical comparison with other reports is also conducted for further study on the TiO2/CdS system for water splitting. (C) 2016 The Electrochemical Society. All rights reserved.
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