Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 138, Issue 32, Pages 10116-10119Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jacs.6b06394
Keywords
-
Categories
Funding
- European Research Council [671093]
- Spanish Government [MAT2015-71842-P, MAT2012-38567-C02-01, SEV-2012-0267]
- Generalitat Valenciana
- Italian project FIR Exploring the Nanoworld
- European Research Council (ERC) [671093] Funding Source: European Research Council (ERC)
Ask authors/readers for more resources
In this work a new ultrafast data collection strategy for electron diffraction tomography is presented that allows reducing data acquisition tithe by one order of Magnitude.,,This Methodology minimizes the radiation damage of, beam-sensitive materials, such as microporous materials. This method, combined with the precession of the electron beam, provides high quality data enabling the determination of very complex structures. Most importantly,, the implementation of this new, electron diffraction methodology is, easily affordable in any modem electron Microscope. As a proof of concept, we have solved a new highly complex zeolitic structure named ITQ-58, with a very low symmetry (triclinic) and a large unit cell volume (1874.61(3)), containing 16 silicon and 32 oxygen atoms in its asymmetric unit, which would be very difficult to solve with the state of the art techniques.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available