4.7 Article

Direct measurement of shear stress for dislocation transferring across {111}?3 grain boundary in aluminum bicrystal via in situ straining TEM

Journal

SCRIPTA MATERIALIA
Volume 221, Issue -, Pages -

Publisher

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.scriptamat.2022.114953

Keywords

Grain boundary; Dislocations; Aluminum; Transmission electron microscopy; In situ experiment

Funding

  1. Japan Society for the Promotion of Science, Japan [16H06366]

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TEM in situ straining was used to study an Al bicrystal with a {111} sigma 3 grain boundary. The activated slip systems and resolved shear stress were determined, and the relationship between grain boundary dislocations and pile-up dislocations was observed.
TEM in situ straining was applied to an Al bicrystal with a {111} sigma 3 grain boundary. The activated slip systems in both grains were determined based on the dislocation line configurations and the crystallographic orientation of the applied load. The resolved shear stress for activation of the dislocation transfer at the GB, tau gb, was directly evaluated from the dislocation motion and the simultaneously obtained stress-strain curve. The evaluated tau gb value agrees with those obtained in a previous study on macroscopic tensile tests. From the geometry of the dislocation reaction, it was presumed that the pile-up lattice dislocations are dissociated into the lattice dislo-cations in the adjacent grain and the GB dislocation. It was determined that the activated slip system in the adjacent grain was dominated by local energetic and geometric conditions rather than the global condition such as the combination of Schmid low and applied stress.

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