Journal
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
Volume 869, Issue -, Pages -Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2022.144508
Keywords
Mg-Mn alloy; Extrusion; Nano precipitates; Superior ductility; Grain boundary sliding
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The study investigated the influence of Mn content (0.4, 0.8, 1.2 wt.%) on the microstructure and mechanical properties of as-extruded dilute binary Mg-Mn alloys. Increasing Mn content resulted in a decrease in the volume fraction and size of dynamically recrystallized (DRXed) grains. Segregation of Mn atoms and nano alpha-Mn dynamical precipitates were observed at the grain boundaries, with the amount of precipitates increasing with Mn content. Tensile tests showed that Mn content significantly affected mechanical properties, with the Mg-0.8 wt.% Mn alloy exhibiting excellent ductility at room temperature.
The effect of Mn content (0.4, 0.8, 1.2 wt. %) on microstructure and mechanical properties of as-extruded dilute binary Mg-Mn alloys was studied. With the increase of Mn content from 0.4 wt. % to 1.2 wt. %, the volume fraction of dynamically recrystallized (DRXed) grains decreases from 89% to 40%, while the DRXed grain size decreases from 3.2 mu m to 1.9 mu m. The segregation of Mn atoms and nano alpha-Mn dynamical precipitates are observed at the grain boundaries of the extruded Mg-0.8Mn alloys and the amount of dynamically precipitates is increased with increasing Mn content. Tensile tests show that the Mn content significantly affects mechanical properties at room temperature (RT). The Mg-0.8 wt. % Mn alloy shows the excellent ductility of 81 % at room temperature in a strain rate of 1 center dot 10(-3) s(-1), the ductility decreases if the Mn content is lower or higher than 0.8 wt. %. The yield strength (YS) and ultimate tensile strength (UTS) increase with increasing Mn content. The large value of strain rate sensitivity exponent (m-value) and small activation volume (V*) of the as-extruded Mg-0.8Mn alloy suggest that grain boundary sliding (GBS) plays an important role in tensile plastic deformation. High volume fraction of the un-DRXed region leads to the reduced contribution of GBS to plastic deformation, decreases ductility at RT. The Atomic force microscopy (AFM) analysis indicates that the contribution of GBS to the total plastic deformation is 2.7 %, 55.1 % and 12.8 % for Mg-0.4Mn, Mg-0.8Mn and Mg-1.2Mn alloys, respectively.
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