Journal
MATERIALS CHARACTERIZATION
Volume 194, Issue -, Pages -Publisher
ELSEVIER SCIENCE INC
DOI: 10.1016/j.matchar.2022.112405
Keywords
Additive manufacturing; Martensitic steel; Electron backscatter diffraction (EBSD); Phase transformation; Microstructure; Texture
Categories
Funding
- Ministry of science and higher education of the Russian Federation [075-152021-690, RF 2296.61321X0030]
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This study focuses on the crystallographic aspects of laser-powder bed fusion of 17-4 PH martensitic steel. The crystallization process showed an epitaxial mechanism and resulted in a specific crystal structure relationship between ferrite and austenite. Grain-boundary austenite was found to have a relationship with adjacent ferrite grains. The phase transformation from austenite to martensite did not exhibit significant variant selection.
Microstructural evolution during laser-powder bed fusion of 17-4 PH martensitic steel was studied. Particular emphasis was paid to the crystallographic aspects of this process. The crystallization of 6-ferrite from the liquid phase was shown to be governed by an epitaxial mechanism which gave rise to the solidification <100> -fiber texture. The austenitic phase preferentially nucleated at the ferrite grain boundaries, while the subsequent migration of phase boundaries was accompanied by extensive annealing twinning. Remarkably, the grain -boundary austenite was related to both adjacent ferrite grains via the Nishiyama-Wasserman orientation rela-tionship. The multiple crystallographic variants associated with the phase transformation and annealing twin-ning resulted in a comparatively weak <110> + <100> -fiber texture in austenite. The subsequent austenite -> martensite phase transformation was governed by the mixed orientation relationship, which included both the Nishiyama-Wasserman and Kurdjumov-Sachs ones. The nearly-random texture in martensite suggested no essential variant selection during the phase transformation.
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