Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 87, Issue 23, Pages 15771-15782Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.2c01734
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Funding
- DST-SERB [CRG/2020/003424]
- SERB-New Delhi
- Praveen Laboratories Pvt. Ltd
- DST-FIST [SR/FST/CSI-270/2015]
- BITS Pilani
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An electrochemical method has been developed to synthesize 2,2-disubstituted indolin-3-ones under mild conditions. A series of nucleophiles have been added to the 2-arylindole-3-ones, generated in situ under metal-free electrochemical oxidative dearomatization of 2-arylindoles, to afford 2,2-disubstituted 3-carbonyl indoles with heteroquaternary centers in 57-79% yields.
An electrochemical method has been developed to synthesize 2,2-disubstituted indolin-3-ones under mild conditions. A series of nucleophiles have been added to the 2-arylindole-3-ones, generated in situ under metal-free electrochemical oxidative dearomatization of 2-arylindoles, to afford 2,2-disubstituted 3-carbonyl indoles with heteroquaternary centers in 57-79% yields.
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