4.7 Article

Investigation of isothermal continuous hot deformation behavior of the new as-cast alumina-forming austenitic alloy

Journal

JOURNAL OF ALLOYS AND COMPOUNDS
Volume 928, Issue -, Pages -

Publisher

ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2022.167236

Keywords

Alumina -forming austenite; As -cast microstructure; Hot deformation; Isothermal; Recrystallization

Funding

  1. Natural Science Foundation of Jiangsu Province [BK20220548]
  2. State Key Lab of Advanced Metals and Materials in University of Science and Technology Beijing [2022-Z21]
  3. China Postdoctoral Science Foundation [2019M661738]
  4. Opening Project of Jiangsu Key Laboratory of Advanced Structural Materials and Application Technology [ASMA202002]

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Multi-pass isothermal continuous hot deformation experiments were conducted to study the grain evolution in the as-cast alumina-forming austenite heat-resistant alloy. The alloys exhibited significant work-hardening characteristics under different deformation conditions, with dynamic recrystallization and static recrystallization occurring. The study confirmed that multi-pass isothermal continuous hot deformation can improve the alloy microstructure and guide industrial production.
Multi-pass isothermal continuous hot deformation experiments were designed for homogenization and recrystallization in the as-cast alumina-forming austenite (AFA) heat-resistant alloy. Flow curves and mi-crostructure characterization were used to study the grain evolution with different deformation parameters in each pass. In particular, attention was paid to the dendrites and segregated phase. Under different hot deformation conditions, the alloys show significant work-hardening characteristics, which result from the strengthening effect of the primary segregated MC-type carbide. The increase in deformation temperature contributes significantly to dynamic recrystallization (DRX), and the main mechanism of DRX is dis-continuous DRX (DDRX). The continuous DRX (CDRX) is less occurring. Static recrystallization (SRX) occurs during the isothermal holding time between deformation passes. SRX becomes more and more apparent with temperature and the holding time. The increase in the deformation passes leads to a gradual dis-appearance of the alloy dendrites and an increase in the recrystallization volume fraction. Meanwhile, the segregated phase gradually decomposes into particles and partially dissolves. However, the segregated phase particles eventually show band-like distribution. SRX grains around the segregated phase will exhibit similar orientations due to particle-stimulated nucleation (PSN) mechanisms. Until the grain size increases to the point that it can escape from particle restraint, it will transform to random orientation. The above study confirms that multi-pass isothermal continuous hot deformation can improve the as-cast micro-structure and guide practical industrial production. (c) 2022 Elsevier B.V. All rights reserved.

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