In Situ Confined Synthesis of a Copper-Encapsulated Silicalite-1 Zeolite for Highly Efficient Iodine Capture

Article Engineering, Environmental

Facile synthesis of novel Bi0-SBA-15 adsorbents by an improved impregnation reduction method for highly efficient capture of iodine gas

Qiang Xian et al.

Summary: The study successfully synthesized Bi-0-SBA-15 for efficient capture of iodine gas, demonstrating excellent capture performance and stability, providing important support for the development of nuclear energy.

JOURNAL OF HAZARDOUS MATERIALS (2022)

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Article Chemistry, Applied

Exploration synthesis and study of indol and pyridine based heterocycle porous organic polytriazine for highly efficient iodine capture

Kuanyu Yuan et al.

Summary: Porous organic polymers (POPs) have shown great potential in the field of volatile radioactive iodine capture due to their porous structures and feasible functional networks. However, the iodine adsorption capacities of POPs still need to be improved through efficient molecule structure design strategy. In this study, a nitrogen-rich porous organic polytrazine (HCPOT-In) was designed and synthesized by a simple one-step Lewis acid-catalyzed reaction. The HCPOT-In exhibited permanent porosity and good stability. With the advantages of its porosity structure, nitrogen-rich skeleton, and pi-conjugated network, HCPOT-In showed excellent volatile iodine adsorption capacity and carbon dioxide capture performance.

JOURNAL OF POROUS MATERIALS (2022)

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Article Multidisciplinary Sciences

Intra-crystalline mesoporous zeolite encapsulation-derived thermally robust metal nanocatalyst in deep oxidation of light alkanes

Honggen Peng et al.

Summary: The study presents a facile strategy to design and synthesize palladium nanoparticles enveloped within a single-crystalline zeolite with intra-mesopores. The resulting material exhibits remarkable performances in light alkane deep oxidation reactions, attributed to the confinement and guarding effect of the zeolite shell and the improvement in mass-transfer efficiency and active metal sites accessibility.

NATURE COMMUNICATIONS (2022)

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Article Nanoscience & Nanotechnology

Role of Zeolite Structural Properties toward Iodine Capture: A Head- to-head Evaluation of Framework Type and Chemical Composition

Brian J. Riley et al.

Summary: This study evaluated zeolite-based sorbents for iodine gas capture and found that Ag-FAU zeolite had the highest adsorption capacity, while Ag-MFI zeolite showed good adsorption capacity and stability in practical applications. The structure and chemical properties of zeolites have an influence on the adsorption performance of iodine from the gas phase.

ACS APPLIED MATERIALS & INTERFACES (2022)

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Article Chemistry, Inorganic & Nuclear

Introducing Zirconium Organic Gels for Efficient Radioiodine Gas Removal

Chuan Tan et al.

Summary: This study found that zirconium-based metal-organic gels (MOGs) exhibit excellent performance in removing radioactive iodine, including good chemical stability and reusability. The increased amount of amino group contributes to the enhanced iodine sorption capacity and kinetics.

INORGANIC CHEMISTRY (2022)

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Article Chemistry, Inorganic & Nuclear

Porous Copper-Loaded Zeolites for High-Efficiency Capture of Iodine from Spent Fuel Reprocessing Off-Gas

Jia Zhou et al.

Summary: This study investigated the adsorption performance of copper-loaded porous zeolites as alternatives to expensive silver-containing zeolites for capturing volatile iodine produced in the nuclear industry. The results showed that copper-loaded zeolites exhibited high iodine adsorption capacities and could adsorb volatile iodine through a chemical mechanism. These copper-loaded zeolites show potential for iodine adsorption application in the nuclear industry.

INORGANIC CHEMISTRY (2022)

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Article Chemistry, Inorganic & Nuclear

Hydrolytically Stable Zr-Based Metal-Organic Framework as a Highly Sensitive and Selective Luminescent Sensor of Radionuclides

Zi-Jian Li et al.

Summary: This study presents a sensitive and selective sensor based on a luminescent Zr-based metal-organic framework for the effective detection of radionuclides UO22+ and I-. The sensor exhibits low detection limits and excellent stability, making it a promising tool for real-world applications.

INORGANIC CHEMISTRY (2022)

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Article Multidisciplinary Sciences

Efficient and simultaneous capture of iodine and methyl iodide achieved by a covalent organic framework

Yaqiang Xie et al.

Summary: The authors demonstrate the simultaneous capture of low-concentration radioactive molecular iodine and organic iodides using a covalent organic framework. The developed material, COF-TAPT, exhibits high crystallinity, a large surface area, and abundant nucleophilic groups, resulting in excellent adsorption capacity for both iodine species.

NATURE COMMUNICATIONS (2022)

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Article Engineering, Environmental

Pitch-based porous polymer beads for highly efficient iodine capture

Guangyuan Chen et al.

JOURNAL OF HAZARDOUS MATERIALS (2022)

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Article Chemistry, Multidisciplinary

Transformation of Porous Organic Cages and Covalent Organic Frameworks with Efficient Iodine Vapor Capture Performance

Chao Liu et al.

Summary: The reaction of BPDDP with cyclohexanediamine results in the synthesis of nitrogen-rich porous organic cage BPPOC and two USTB-1 and USTB-2 COFs. The newly prepared COFs show enhanced iodine vapor adsorption capability and can be transformed between different structures by exchanging the imine unit. This transformation is influenced by the crystal structures and the porosity of the materials, with nitrogen atoms proving superior to sulfur atoms for POCs in iodine vapor capture.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2022)

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Article Engineering, Environmental

Novel synthesis of NaY-NH4F-Bi2S3 composite for enhancing iodine capture

Mei Jiang et al.

Summary: In this study, a novel fluoride modified bismuth sulfide supported NaY zeolite material was reported for the effective capture of radioactive iodine in spent fuel reprocessing. The material exhibited high sorption capacity, excellent thermal stability, and radiation stability, making it a potential candidate for capturing and immobilizing radioactive gaseous iodine.

CHEMICAL ENGINEERING JOURNAL (2022)

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Review Chemistry, Multidisciplinary

Adsorption of iodine in metal-organic framework materials

Xinran Zhang et al.

Summary: Nuclear power will continue to provide energy, but there are challenges in waste disposal and radioactive release. MOF materials show potential for selective adsorption of iodine and improving adsorption performance.

CHEMICAL SOCIETY REVIEWS (2022)

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Article Chemistry, Multidisciplinary

Boosting the Iodine Adsorption and Radioresistance of Th-UiO-66 MOFs via Aromatic Substitution

Zi-Jian Li et al.

Summary: The study found that the electron-donating amino group has a positive impact on the adsorption of iodine in both solution and vapor states, with the di-substituted Th-UiO-66-(NH2)2 showing excellent removal rate and uptake capacity for iodine. Additionally, the radiolytic stability of MOFs was investigated, leading to the discovery of Th-UiO-66-NH2 as one of the most radioresistant MOFs reported to date.

CHEMISTRY-A EUROPEAN JOURNAL (2021)

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Article Water Resources

Release of toxic methylene blue from water by mesoporous silicalite-1: characterization, kinetics and isotherm studies

Sabarish Radoor et al.

Summary: In this study, a mesoporous silicalite-1 was developed using CMC as a template for the removal of MB from aqueous solution. The synthesized silicalite-1 was characterized through various methods and the adsorption parameters for the removal of MB dye were investigated. The results showed that the developed silicalite-1 exhibited efficient removal of MB dye and maintained high removal efficiency even after multiple adsorption-desorption cycles.

APPLIED WATER SCIENCE (2021)

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Article Engineering, Chemical

Kinetics of aging process on reduced Ag exchanged mordenite in dry air and humid air

Seungrag Choi et al.

Summary: The aging effects of dry air and humid air on reduced silver exchanged mordenite (Ag(0)Z) were studied. It was found that iodine loading capacity decreased with increasing aging temperatures, time, and water vapor concentrations. The oxidation of Ag-0 was identified as the rate determining step in the aging process.

AICHE JOURNAL (2021)

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Article Engineering, Environmental

Efficient removal and immobilization of radioactive iodide and iodate from aqueous solutions by bismuth-based composite beads

Qian Zhao et al.

Summary: A stable millimeter-level bismuth-based polymer composite bead was developed for effectively removing radioactive iodine from aqueous solutions, showing high adsorption capacities and selective removal of iodine anions. The composite bead demonstrated efficient removal kinetics, reduced leaching, and easy separation, making it a promising candidate for environmental remediation of iodine-contaminated water.

CHEMICAL ENGINEERING JOURNAL (2021)

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Article Chemistry, Multidisciplinary

Platelike MFI Crystals with Controlled Crystal Faces Aspect Ratio

Weijiong Dai et al.

Summary: A simple synthetic strategy was developed to reduce the thickness of zeolite crystals along the b-axis, providing a short diffusion path along the straight channel. The synthesized MFI crystals, with micrometer-size along the a- and c-axis and thickness in the tens of nanometers along the b-axis, showed good catalytic activity in the methanol-to-hydrocarbons reaction. The synthesis of platelike MFI crystals was successfully scaled up to a kilogram scale, demonstrating extended catalytic lifetime compared to commercial nanosized samples.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2021)

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Article Chemistry, Applied

Synthesis of N-containing porous aromatic frameworks via Scholl reaction for reversible iodine capture

Jian Wang et al.

Summary: Three porous organic frameworks (POFs) were constructed via a cost-effective Scholl reaction with N-containing building units, showing moderate porosity and satisfactory thermal stability. The electron-rich amino group in the POFs improved the affinity to iodine, achieving iodine uptake capacities superior to most porous adsorbents. The promising and cost-effective materials could be used for nuclear waste management applications.

MICROPOROUS AND MESOPOROUS MATERIALS (2021)

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Article Chemistry, Applied

Synthesis of nitrogen-containing covalent organic framework with reversible iodine capture capability

Run Chen et al.

Summary: This study explored the crystallization of a stable nitrogen-containing COF for efficient and reversible volatile iodine capture, demonstrating high uptake capacity and recyclability.

MICROPOROUS AND MESOPOROUS MATERIALS (2021)

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Article Agricultural Engineering

High iodine adsorption by lignin-based hierarchically porous flower-like carbon nanosheets

Zihao Ma et al.

Summary: Efficient adsorbents based on lignin-derived graphene flower-like carbon nanosheets have been developed for capturing and adsorbing radioactive iodine in air and aqueous solutions during nuclear disposal and accidents. By adjusting the activation methods, different pore size structures in the carbon nanosheets were achieved, resulting in excellent iodine adsorption capacities in various environments.

INDUSTRIAL CROPS AND PRODUCTS (2021)

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Article Chemistry, Multidisciplinary

A nitrogen-rich covalent organic framework for simultaneous dynamic capture of iodine and methyl iodide

Linwei He et al.

Summary: A new design philosophy involving a nitrogen-rich covalent organic framework material with enhanced specific host-guest interactions has been proposed for the simultaneous capture of both iodine gas and organic iodide. This material shows an ultrahigh uptake capacity under static sorption conditions and record-high iodine loading capability under dynamic conditions.

CHEM (2021)

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Article Chemistry, Physical

Effect of Metal Ion Modified TS-1 on Cyclization Properties of 6-Hydroxyhexanoic Acid

Xuanying Cheng et al.

Summary: In this study, TS-1 samples modified by different metal ions were prepared using the equal volume impregnation method and applied to the cyclization reaction of 6-hydroxyhexanoic acid. It was found that Mg2+ and Co2+ modification increased the yield of epsilon-caprolactone, while Zn2+ modification decreased the yield.

CATALYSIS LETTERS (2021)

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Enhanced performances of bimetallic Ga-Pt nanoclusters confined within silicalite-1 zeolite in propane dehydrogenation

Yansu Wang et al.

Summary: Bimetallic Ga-Pt nanocatalysts encapsulated into silicalite-1 zeolites were synthesized for propane dehydrogenation, showing high activity, selectivity, and stability. The confined GaPt alloy nanoclusters act as active sites, exhibiting a high propene selectivity and formation rate. The zeolite encapsulation enhances regeneration stability, maintaining catalytic activity over multiple cycles.

JOURNAL OF COLLOID AND INTERFACE SCIENCE (2021)

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Host-guest interaction-mediated nanointerface engineering for radioiodine capture

Juan Wang et al.

Summary: Nuclear power plants are rapidly expanding worldwide to meet energy demands, with research focusing on capturing volatile radioiodine effectively. Understanding the binding mechanism at the gas-solid interface is crucial for constructing high-performance adsorbents. Recent studies highlight the importance of optimizing interface properties and binding sites to regulate host-guest interactions.

NANO TODAY (2021)

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Novel bismuth-based electrospinning materials for highly efficient capture of radioiodine

Zhenjiang Tian et al.

Summary: This study reported three novel bismuth-based iodine sorption materials with improved iodine capture capacities. Through hydrothermal treatment, active sites appeared on the fiber surface, enhancing the efficiency of iodine gas contact. The experimental results showed that the coating on the fiber surface significantly increased the iodine adsorption capacity, with elemental bismuth demonstrating a higher effective atomic utilization rate.

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Cu/Cu2O-immobilized cellulosic filter for enhanced iodide removal from water

Jaeyoung Seon et al.

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Performance of radio-iodine discharge control methods of nuclear reprocessing plants

K. Umadevi et al.

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Comprehensive comparison of bismuth and silver functionalized nickel foam composites in capturing radioactive gaseous iodine

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Self-assembled iron-containing mordenite monolith for carbon dioxide sieving

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Visualization of gaseous iodine adsorption on single zeolitic imidazolate framework-90 particles

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Encapsulation of CuO nanoparticles within silicalite-1 as a regenerative catalyst for transfer hydrogenation of furfural

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Rapid iodine capture from radioactive wastewater by green and low-cost biomass waste derived porous silicon-carbon composite

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In Situ Confined Synthesis of a Copper-Encapsulated Silicalite-1 Zeolite for Highly Efficient Iodine Capture

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