4.6 Article

Bubble Morphology Analysis and Pressure Drop of Gas-Liquid Two-Phase Flow inside a Quarto Static Mixer

Journal

INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH
Volume 61, Issue 50, Pages 18574-18587

Publisher

AMER CHEMICAL SOC
DOI: 10.1021/acs.iecr.2c03917

Keywords

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Funding

  1. Key Scientific Research Project of Education Department of Liaoning Province [LJKZ0429, LJKMZ20220773]
  2. Shenyang Young and Middle-aged Science and Technology Innovation Talent Support Program [RC200032]
  3. National Natural Science Foundation of China [21476142]
  4. Distinguished Professor of Liaoning Province [LCH[2018]35]
  5. Natural Science Foundation of Liaoning Province [2022-MS-290]
  6. Talent Introduction Research Fund of China University of Petroleum (East China) [R20220113]

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This study experimentally investigates the effect of upward two-phase flow in industrial static mixers on dispersion mixing. Empirical correlations and dimensionless correlations are proposed to assess the dispersion performance and gas-liquid pressure drop in the mixer. The critical velocities for flow pattern transition are identified using pressure fluctuation analysis. Additionally, the quantitative effect of gas velocity on frequency and power spectral density function is analyzed.
The upward two-phase flow in vertical static mixers is beneficial for dispersion mixing. The bubble size distribution, aspect ratio, and angle distribution of the dispersed phase at various superficial liquid/gas velocities in an industrial Quarto static mixer (QSM) are experimentally studied. The dispersion performance of the QSM is assessed by Sauter mean diameter (d32), and the empirical correlation of axial d32 distribution is proposed. The gas-liquid pressure drop in the QSM is measured under UL = 0-0.071 and UG = 0-0.042 m/s, and two new dimensionless empirical correlations are proposed. Based on pressure fluctuation signal time series, the standard deviation, kurtosis, and skewness are analyzed, and the inlet and outlet critical velocities of flow pattern transition from pseudo-homogeneous to heterogeneous in the QSM are identified. Finally, the effect of UG on the dominant frequency and power spectral density function is quantitatively analyzed at the inlet and outlet sections.

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