Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 81, Issue 3, Pages 1244-1250Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b02535
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Funding
- National Natural Science Foundation of China [21402243, 81522041, 81373258]
- Fundamental Research Funds for the Central Universities (Sun Yat-sen University) [13ykpy09]
- Medical Scientific Research Foundation of Guangdong Province [B2014105]
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A palladium-catalyzed oxidative C-H bond decarboxylative acylation of N-nitrosoanilines using alpha-oxocarboxylic acid as the acyl source is described. The catalyst Pd(OAc)(2) and oxidant (NH4)(2)S2O8 enabled ortho-acylation of N-nitrosoanilines at room temperature, affording an array of N-nitroso-2-aminobenzophenones in moderate to excellent yields.
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