Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 81, Issue 7, Pages 2713-2729Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b02475
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Funding
- Department of Science and Technology [IFA12-CH-22]
- University Grants Commission India
- Agencia de Ciencia y Tecnologia de la Region de Murcia [19278/PI/14]
- MINECO-Programa Estatal de I+D+i Orientada a los Retos de la Sociedad [CTQ2015-67927-R]
- Alexander von Humboldt Foundation
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A broadly applicable catalyst system consisting of water-soluble Pd-imidate complexes has been enployed for the Suzuki-Miyaura cross-coupling of four different nucleosides in water under mild conditions. The efficient nature of the catalyst system also allowed its application in developing a microwave-assisted protocol with the purpose of expediting the catalytic reaction. Preliminary mechanistic studies, assisted by catalyst poison tests and stoichiometric tests performed using an electrospray ionization spectrometer, revealed the possible presence of a homotopic catalyst system.
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