Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 81, Issue 10, Pages 4371-4377Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.6b00473
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- French Agence Nationale de la Recherche (ANR) [ANR-13-JS07-0008]
- Centre National de la Recherche Scientifique (CNRS)
- Agence Nationale de la Recherche (ANR) [ANR-13-JS07-0008] Funding Source: Agence Nationale de la Recherche (ANR)
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The first umpolung addition/intramolecular Wittig reaction, catalytic in phosphine, is described. The in situ phosphine oxide reduction was accomplished by the use of silane and a catalytic amount of bis(4-nitrophenyl)phosphate. This catalytic protocol is applicable to the synthesis of a wide range of functionalized 9H-pyrrolo[1,2-a]indoles and pyrrolizines (18 examples, 70-98% yields).
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