Journal
CATALYSIS LETTERS
Volume 146, Issue 1, Pages 117-125Publisher
SPRINGER
DOI: 10.1007/s10562-015-1659-4
Keywords
Microwave; Palladium nanoparticle; Metal-organic frameworks; Suzuki-Miyaura coupling reaction
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Funding
- National Natural Science Foundation of China [31171698, 31471643]
- Innovation Research Program of Department of Education of Hebei for Hebei Provincial Universities [LJRC009]
- Natural Science Foundation of Hebei Province [B2015204003]
- Natural Science Foundation of Agricultural University of Hebei [ZD201506, LG201404]
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In this paper, the palladium nanoparticles were successfully encapsulated in metal-organic framework material, UiO-66, by a facile approach. Based on the microwave-assisted method, the pores of UiO-66 were activated and the metal precursors were reduced at the same time in the presence of reducing agent. The obtained Pd@UiO-66 was characterized via transmission electron microscopy, powder X-ray diffraction, N-2 adsorption and X-ray photoelectron spectroscopy. The Pd@UiO-66 exhibited efficient catalytic activity for the Suzuki-Miyaura coupling reactions at mild condition. [GRAPHICS] .
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