Fatigue performance of laser powder bed fusion hydride-dehydride Ti-6Al-4V powder

Hydride-dehydride (HDH) Ti-6Al-4V alloy with particle size distribution of 50-120 mu m is laser powder bed fusion (L-PBF) processed using optimum processing parameters and a near-fully dense structure with a density of 99.9 % is achieved. Microstructural observations and phase analyses indicate formation of columnar beta grains with acicular alpha/alpha ' phases in as-built condition. The roughness of the as-fabricated samples is significant with an average roughness of R-a = 15.71 +/- 3.96 mu m and a root mean square roughness of R-rms = 108.4 +/- 24.9 mu m, however, both values are reduced to R-a = 0.19 +/- 0.04 mu m and R-rms = 4.9 +/- 0.6 mu m after mechanical grinding. Mechanical tests are carried out on as-fabricated specimens followed by stress relief treatment. All samples are tested to failure in fatigue, under fully-reversed tension-compression conditions of R = -1. The as-built samples failed from the surface with crack initiation mainly at micro-notches, whereas after mechanically grinding, crack initiation changed to subsurface defects such as pores. Minimizing surface roughness by mechanically grinding eliminates surface micro-notches which improves fatigue strength in the high cycle fatigue region. Fatigue notch factor calculations showed that the effect of surface roughness was significantly lower when HDH powder is used compared to standard spherical powder. X-ray diffraction analysis revealed an in-plane compressive stress, micro-strain and grain refinement on the surface of the mechanically ground samples. Fractography observations (macroscale) revealed a fully brittle fracture in the first stage of crack growth with a transition to a dominantly ductile fracture in the third stage of crack growth. On the other hand, at the micro scale, even the brittle fracture regions showed evidence of ductile fracture within the alpha ' martensite laths.

Automated summary

L-PBF processed HDH Ti-6Al-4V alloy achieves near-full density with a particle size distribution of 50-120 μm. Mechanical grinding reduces surface roughness and improves fatigue strength. Fracture behavior shows a combination of brittle and ductile fractures.