4.7 Article

Microstructure evolution and mechanical properties of industrial scale samples of Mg-Gd-Y-Zn-Zr alloy after repetitive upsetting-extrusion process

Journal

JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
Volume 21, Issue -, Pages 2013-2027

Publisher

ELSEVIER
DOI: 10.1016/j.jmrt.2022.10.038

Keywords

Repetitive upsetting-extrusion (RUE); Mg-9Gd-3Y-2Zn-0; 4Zr alloy; Microstructure evolution; Mechanical properties; Strengthening

Funding

  1. National Natural Science Foundation of China [52075501, 2019D111146]
  2. Natural Science Foundation of Shanxi Province [2019D111146]
  3. Bureau of science, technology and industry for National Defense of China [WDZC2019JJ006]
  4. Key R&D program of Shanxi Province [201903D421036]
  5. Magnesium alloy highperformance XXX multi-directional extrusion technology [JCKY2018408B003]
  6. special fund for Science and Technology Innovation Teams of Shanxi Province

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This paper comprehensively investigates the microstructure evolution and mechanical properties of industrial-scale Mg alloys. The results reveal heterogeneous microstructure and anisotropic texture and mechanical properties of the RUEed samples. The edge region along the extrusion direction shows superior tensile strength due to smaller grain size and higher area fraction of dynamic recrystallized grains.
As one of the severe plastic deformation (SPD) methods, repetitive upsetting-extrusion (RUE) technique was an effective way to refine grains for large-sized billet at blank -making stage. The microstructure evolution and mechanical properties of industrial -scale Mg-9Gd-3Y-2Zn-0.4Zr (wt.%) alloys were comprehensively investigated in this paper. The experimental alloys exhibited heterogeneous microstructure in the different regions and directions due to the uneven deformation temperature and strain during the RUE deformation process. In addition, the texture and mechanical properties of the RUEed samples also exhibited obvious anisotropy. In particular, the RUEed sample in the edge region along extrusion direction (EED) showed a superior tensile strength with ultimate tensile strength (UTS) of 357 MPa, tensile yield strength (TYS) of 242 MPa and the failure elongation (FE) of 9.0%, due to the smaller average grain size (12.7 mm) and higher area fraction of the dynamic recrystallized (DRXed) grains (82.2%) than other regions. Further-more, the results also exhibited that the enhancement of the mechanical properties of the RUEed samples were mainly attributed to Hall-Petch strengthening, Orowan strength-ening and texture strengthening.(c) 2022 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

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