Journal
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
Volume 20, Issue -, Pages 4130-4136Publisher
ELSEVIER
DOI: 10.1016/j.jmrt.2022.09.006
Keywords
Additive manufacturing; Revised Hall-Petch relationship; Grain size distribution; Materials characterization
Funding
- Structural Metal Alloy Program (SMAP) [A18b1B0061]
- Agency for Science, Technology and Research in Singapore
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The study compared EBSD and OM techniques, investigated the effects of different parameters on results, and proposed a modified Hall-Petch equation considering grain size distributions for almost all AM alloy systems with remarkable agreement between predicted strength and experimental values.
Additively manufactured (AM) metal alloys normally exhibit very diverse grain size distri-butions. The size measured by electron backscatter diffraction (EBSD) is generally smaller than that from optical microscope (OM) due to better resolution, but proper scan setup must be chosen to reveal the existing fine grains. In this work, we compared these two widely applied techniques and investigated the effects of different parameters on the resulting average diameter d. Regarding the discrepancies of parameters in the literatures, a standard EBSD setup is suggested, so that >99% of the total grain area should be detected. The grain distribution characteristics for AM fabricated alloys were also illustrated. A simply modified Hall-Petch equation is proposed by considering the grain size distributions using grains covering >99% of the measured area. It gives remarkable agreement between predicted strength and experimental values for almost all the AM alloy systems we tested, which possess very diverse grain size distributions. This revised model can extend to other AM alloys with heterogeneous microstructures and is very practical for engineering approach.(c) 2022 The Author(s). Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
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